Data File D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.DSample Name: BIZ2015-508-DJL2=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 25Acq. Instrument : HY-LCMS-02 Location : P1-C-05Injection Date : 5/8/2015 10:48:52 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/8/2015 9:05:04 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\1.MLast changed : 5/8/2015 5:22:40 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-N0583 Batch#15984 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.D) 1.755 1.440 1.519 1.599 1.919mAU1200100080060040020000.511.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.440 MM 0.0519 7.54738 2.42219 0.1929 2 1.519 MM 0.0715 7.44159 1.73462 0.1902 3 1.599 MM 0.0672 8.78491 2.17786 0.2245 4 1.755 MM 0.0446 3884.77466 1452.99280 99.2911 5 1.919 MM 0.0447 3.96074 1.47570 0.1012 Totals : 3912.50928 1460.80316 ===================================================================== *** End of Report ***HY-LCMS-02 5/8/2015 5:22:42 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.DSample Name: BIZ2015-508-DJL2============================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 25Acq. Instrument : HY-LCMS-02 Location : P1-C-05Injection Date : 5/8/2015 10:48:52 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/8/2015 9:05:04 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\METHOD\\1.MLast changed : 5/8/2015 5:24:13 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-N0583 Batch#15984 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.D) ES-API, Pos, Sca 1.747250000200000150000100000500000.511.522.53min HY-LCMS-02 5/8/2015 5:24:15 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.DSample Name: BIZ2015-508-DJL2MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.747 1059395 747.90 I 746.80 I 425.90 I 384.90 I 363.90 I 362.95 I*MSD1 SPC, time=1.726:1.762 of D:\\AGLIENT 1260\\DATA\\20150508\\20150508 2015-05-08 09-05-04\\BIZ2015-508-DJL2.D ES-API,10080 746.8 363.0Max: 709896040 363.9 425.90100200300400500600700800900m/z *** End of Report ***HY-LCMS-02 5/8/2015 5:24:15 PM Li Shan(LCMS-02) 426.920 384.9 400.9 748.8 747.9Page 2 of 2